Carbon 14 dating denotes the
All laboratories examined the textile samples microscopically to identify and remove any foreign material.The Oxford group cleaned the samples using a vacuum pipette, followed by cleaning in petroleum ether (40° C for 1 h) to remove lipids and candlewax, for example.The second pair of subsamples was treated with a commercial detergent (1.5% SDS), distilled water, 0.1% HCL and another detergent (1.5% triton X-100); they were then submitted to a Soxhlet extraction with ethanol for 60 min and washed with distilled water at 70° C in an ultrasonic bath (method b).The Oxford group divided the precleaned sample into three.Photography of the shroud by Secondo Pia in 1898 indicated that the image resembled a photographic 'negative' and represents the first modern study.Subsequently the shroud was made available for scientific examination, first in 19 by a committee appointed by Cardinal Michele Pellegrino .At the same time, the British Museum was invited to help in the certification of the samples provided and in the statistical analysis of the results. The age of the shroud is obtained as AD 1260-1390, with at least 95% confidence. The three containers containing the shroud (to be referred to as sample 1) and two control samples (samples 2 and 3) were then handed to representatives of each of the three laboratories together with a sample of the third control (sample 4), which was in the form of threads.The procedures for taking the samples and treating the results were discussed by representatives of the three chosen laboratories at a meeting at the British Museum in January 1988 and their recommendations = standard deviation) errors, of the Shroud of Turin and control samples, as supplied by the three laboratories (A, Arizona; O, Oxford; Z, Zurich) (See also Table 2.) The shroud is sample 1, and the three controls are samples 2-4. The sampling of the shroud took place in the Sacristy at Turin Cathedral on the morning of 21 April 1988. All these operations, except for the wrapping of the samples in foil and their placing in containers, were fully documented by video film and photography.
The Shroud of Turin , which many people believe was used to wrap Christ's body, bears detailed front and back images of a man who appears to have suffered whipping and crucifixion.
Following this intercomparison, a meeting was held in Turin in September-October 1986 at which seven radiocarbon laboratories (five AMS and two small gas-counter) recommended a protocol for dating the shroud. The samples were then taken to the adjacent Sala Capitolare where they were wrapped in aluminium foil and subsequently sealed inside numbered stainless-steel containers by the Archbishop of Turin and Dr Tite.
In October 1987, the offers from three AMS laboratories (Arizona, Oxford and Zurich) were selected by the Archbishop of Turin, Pontifical Custodian of the shroud, acting on instructions from the Holy See, owner of the shroud. Samples weighing 50 mg from two of the three controls were similarly packaged.
Each subsample was treated with 1M HCL (80° C for 2h), 1M Na OH (80° C for 2 h) and again in acid, with rinsing in between.
Two of the three samples were then bleached in Na OCL (2.5% at p H-3 for 30 min).
Testore of Department of Materials Science, Turin Polytechnic and G. If the samples had been unravelled or shredded rather than being given to the laboratories as whole pieces of cloth, then it would have been much more difficult, but not impossible, to distinguish the shroud sample from the controls.